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Toketsushiryokokansochi

机译:呕血思想thought措施

摘要

PURPOSE:To observe a sample in its original form, by providing a cryogen storage section around the held sample to fit the sample to a sample exchanger for an electron microscope. CONSTITUTION:A body 23 and a holder 24 are removed from a bearer 22 secured to the sample excahnge chamber 9 of a electron microscope or the like. Liquefied nitrogen or the like is injected into a cryogen storage section 44 defined by a bellows 43. A sample cylinder 4 holding a frozen sample is attached to the top of the body 23 in such a manner that the cylinder is cooled by the cryogen. The body 23 is fitted to the bearer 22. The sample exchange chamber 9 is evacuated of gas. The sample is thereafter protruded into the chamber 9, grasped by the grabber of an exchange rod, moved to a sample mounting position in the electron microscope or the like and mounted in the position. The moisture of the sample is thus kept from being evaporated, so that the sample is prevented from being deformed. Therefore, the sample can be observed in its original form.
机译:目的:通过在保存的样品周围提供冷冻剂存储部分,以使样品适合电子显微镜的样品交换器,以观察原始形式的样品。组成:从固定在电子显微镜或类似物的样品传送腔9上的支架22上取下主体23和支架24。液化的氮气等被注入到由波纹管43限定的制冷剂存储部分44中。保持冷冻样品的样品瓶4以这样的方式附接到主体23的顶部,使得该瓶被制冷剂冷却。主体23安装在承载架22上。样品交换室9被抽空。此后,将样品突出到腔室9中,该腔室9被交换杆的抓取器抓住,移动到电子显微镜等中的样品安装位置并安装在该位置。因此,防止了样品的水分蒸发,从而防止了样品变形。因此,可以以其原始形式观察样品。

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