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Process for the treatment of petroleum fractions containing metals, in the presence of solid particles, including a magnetohydrostatic separation stage for the said particles and the recycling of part of them

机译:在固体颗粒的存在下处理含金属的石油馏分的方法,包括用于所述颗粒的静磁静水分离阶段和其中一部分的再循环

摘要

Process for the treatment of a hydrocarbon fraction containing metals and comprising the following stages: (a) the said hydrocarbon fraction is treated in the presence of mean density particles (d.sub.o) under conditions for eliminating at least partly the metals contained therein and deposits of said metals on at least one fraction of said solid particles; (b) at least part of the solid particles from stage (a), whose mean density is (d.sub.i) is drawn off; (c) said solid particles from stage (b) are magnetohydrostatically separated by introducing said solid particles into a ferrofluid placed in a non-uniform magnetic field and creating a vertical magnetic field, whose intensity is adjusted in such a way that the apparent mean density (d.sub.af) of the ferrofluid permits the separation of said solid particles into at least one mean density fraction (d.sub.i) below said apparent mean density (d.sub.af) of the ferrofluid and into at least one mean density fraction (d.sub.s) above said mean apparent density (d.sub.af) of the ferrofluid and above the mean density (d.sub.1) of the solid particles drawn off in stage (b); (b) at least one fraction of said mean density solid particles (d.sub.s) is recovered; and (e) recycling takes place to stage (a) of at least one fraction of said mean density solid particles (d.sub.i). The solid particles preferably comprise particles of a catalyst and the treatment is e.g. a hydrotreatment.
机译:处理包含金属并包括以下步骤的烃馏分的方法:(a)在至少部分消除其中所含金属的条件下,在平均密度颗粒(d.sub.o)存在下处理所述烃馏分。所述金属沉积在至少一部分所述固体颗粒上; (b)抽出至少部分来自阶段(a)的平均密度为(d.sub.i)的固体颗粒; (c)通过将所述固体颗粒引入放置在非均匀磁场中的铁磁流体中并产生垂直磁场,从而将来自步骤(b)的所述固体颗粒进行静磁静水分离,其强度以表观平均密度的方式进行调节。铁磁流体(daf)允许将所述固体颗粒分离成低于铁磁流体的所述表观平均密度(daf)的至少一个平均密度分数(di)和至少在所述铁磁流体的所述平均表观密度(daf)之上和在步骤(b)中排出的固体颗粒的平均密度(dsub)之上一个平均密度分数(ds); (b)回收至少一小部分所述平均密度固体颗粒(d.s.); (e)将至少一小部分所述平均密度固体颗粒(d.sub.i)再循环到(a)阶段。固体颗粒优选地包含催化剂颗粒,并且处理例如为H 2 O 3。加氢处理。

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