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A method for the production of meso - carbon micro spheres.

机译:一种生产中碳微球的方法。

摘要

A process for producing a reformed pitch useful for various carbon materials is provided. This process com­prises mixing a pitch having a ratio of aromatic hydrocar­bon fa of 0.6 or more with a Lewis acid and a co-solvent so as to give a mol ratio of the said Lewis acid to the said pitch in the range of 0.3 ∼ 5.0 and a mol ratio of the said co-solvent to the said pitch in the range of ratio of 2.5 ∼ 50, reacting the mixture at a temperature of 100 ∼ 300°C and removing the Lewis acid and the co-­solvent from the reaction product. Meso-Carbon microbeads having a uniform diameter of 20µm or less can be produced at a high yield of 60% or more by heat treating the reformed pitch at 200 ∼ 380°C to produce the optically anisotropic small spheres and separating them from an op­tically isotropic matrix.
机译:提供了一种用于各种碳材料的重整沥青的生产方法。该方法包括将具有0.6或更高的芳烃fa比率的沥青与路易斯酸和助溶剂混合,以使所述路易斯酸与所述沥青的摩尔比在0.3〜5.0的范围内,并且所述助溶剂与所述沥青的摩尔比在2.5〜50的范围内,使混合物在100〜300℃的温度下反应,并从反应产物中除去路易斯酸和助溶剂。通过在200〜380°C热处理重整沥青以生产光学各向异性的小球并将其与光学各向同性分离,可以以60%或更高的高产率生产具有20μm或更小的均匀直径的中碳微珠。矩阵。

著录项

  • 公开/公告号DE68917318T2

    专利类型

  • 公开/公告日1995-02-09

    原文格式PDF

  • 申请/专利权人 PETOCA LTD JP;

    申请/专利号DE1989617318T

  • 发明设计人 TAMAKI TOSHIO JP;

    申请日1989-05-12

  • 分类号C10C1/00;C10C3/00;

  • 国家 DE

  • 入库时间 2022-08-22 04:08:34

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