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METHOD OF PREPARING CATALYST FOR HYDROGENATION OF BENZOIC ACID INTO CYCLOHEXANECARBOXYLIC ACID

机译:苯加氢加氢制环己烷羧酸催化剂的制备方法

摘要

FIELD: catalysts for organic syntheses. SUBSTANCE: method consists in impregnating carbon carrier with aqueous solution of palladium-hydrochloric acid and sodium carbonate, reducing palladium with sodium formate with subsequent washing, drying, impregnation with sodium carbonate solution, and redrying. Novelty consists in using, as carrier, porous pyrolytic carbon in the form of hollow globules 500-5000 in size, specific surface area 75-640 sq. m/g, and average interfacial distance 3.4-3.6 . EFFECT: increased catalytic activity.
机译:领域:有机合成的催化剂。实质:该方法包括用钯-盐酸和碳酸钠的水溶液浸渍碳载体,用甲酸钠还原钯,随后洗涤,干燥,用碳酸钠溶液浸渍和再干燥。新颖之处在于使用空心球形式的多孔热解碳作为载体500-5000 的大小,比表面积75-640平方米/克,平均界面距离3.4-3.6 <图像文件=” 00000004.GIF“ he =” 6“ id =” imag0.4 “ imgContent =” undefined“ imgFormat =” GIF“ wi =” 2“ />。效果:增加催化活性。

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