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SODIUM-PHENOL-WATER ORTHOHYDROXYMANDELATE COMPLEX, PREPARATION METHOD AND USE FOR ISOLATION OF SODIUM ORTHOHYDROXYMANDELATE

机译:苯酚-水-羟基扁桃酸钠钠配合物,制备方法及其在邻苯二酚-羟基扁桃酸钠的分离中的用途

摘要

P A crystallized sodium-phenol-water orthohydroxymandelate complex, its preparation process in which phenol (P2) is introduced into an aqueous solution S at a pH between 7 and 9.5 to obtain the expected product crystallized, the aqueous solution S being such that resulting from the reaction of phenol (P1) on glyoxylic acid in the presence of a tertiary amine and a trivalent cation, then treatment using a solution d 'an alkali hydroxide, application of this complex to the preparation of sodium orthohydroxymandelate (OHMNa), process for the preparation of the latter from the starting complex. /P
机译:

结晶的钠-苯酚-水原羟基扁桃酸盐复合物,其制备方法是将苯酚(P2)引入pH 7至9.5的水溶液S中以获得结晶的预期产物,水溶液S使得在叔胺和三价阳离子存在下,苯酚(P1)与乙醛酸反应生成的产物,然后用碱金属氢氧化物溶液处理,将该配合物应用于原羟基扁桃酸钠(OHMNa)的制备过程用于从起始复合物中制备后者。

著录项

  • 公开/公告号FR2739618A1

    专利类型

  • 公开/公告日1997-04-11

    原文格式PDF

  • 申请/专利权人 SOCIETE FRANCAISE HOECHST;

    申请/专利号FR19950011658

  • 发明设计人 CHRISTIAN SIDOT;MICHEL TARLIER;

    申请日1995-10-04

  • 分类号C07C59/52;C07C39/04;

  • 国家 FR

  • 入库时间 2022-08-22 03:12:11

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