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Process for preparing non vitrified homopolymers of methyl methacrylate having low residual monomer contents
Process for preparing non vitrified homopolymers of methyl methacrylate having low residual monomer contents
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机译:制备具有低残留单体含量的甲基丙烯酸甲酯的非玻璃化均聚物的方法
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摘要
The prodn. of unvitrified methyl methacrylate (MMA) homo- or co-polymers with a low residual monomer content (I) comprises: (a) prepn. of a dispersion of an emulsion polymer of MMA and opt. up to 50 wt.% comonomer (II); (b) reducing the residual monomer content by adding more polymerisation initiator and heating; and (c) spray drying at a temp. above the b.pt. of MMA or above that of any comonomer present with a higher b.pt. than MMA. Also claimed is unvitrified spray-dried PMMA emulsion polymer (I) contg. less than 5 wt.% comonomer, with a residual monomer content of not more than 50 (pref. not more than 30) ppm as obtd. by this process.
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