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Apparatus for X-ray analysis in grazing exit conditions

机译:放牧出境条件下的X射线分析设备

摘要

In order to achieve suitable positional resolution for an angular scan in Grazing Exit X-ray Fluorescence (GEXRF), the sample (2) should be irradiated with a small spot (14). Consequently, the fluorescent radiation yield is low so that the duration of a measurement is comparatively long. In order to mitigate this drawback, the invention proposes the use of an analyzing X-ray mirror (16) having a line focus (22) extending perpendicularly to the sample surface (4). The line focus (22) coincides with a line-shaped PSD (24), so that every position on the PSD corresponds to a given height on the mirror, which height itself corresponds to a given take-off angle of the fluorescent radiation relative to the sample surface. Excellent positional resolution and an attractive fluorescent radiation yield are obtained by irradiating the sample by way of a focused electron beam.
机译:为了在放牧X射线荧光(GEXRF)中获得适合角度扫描的位置分辨率,应该对样品( 2 )照射一个小点( 14 )。因此,荧光辐射产率低,使得测量持续时间相对较长。为了减轻该缺点,本发明提出使用分析X射线镜( 16 ),该分析X射线镜具有垂直于样品表面( 22 )的线焦点( 22 )。 4 )。线焦点( 22 )与线形PSD( 24 )重合,因此PSD上的每个位置都对应于镜子上的给定高度,该高度本身对应于荧光辐射相对于样品表面的给定起飞角。通过用聚焦电子束辐照样品,可以获得极好的位置分辨率和诱人的荧光辐射产率。

著录项

  • 公开/公告号US6263042B1

    专利类型

  • 公开/公告日2001-07-17

    原文格式PDF

  • 申请/专利权人 U.S. PHILIPS CORPORATION;

    申请/专利号US19990406285

  • 发明设计人 PIETER K. DE BOKX;SANDER G. DEN HARTOG;

    申请日1999-09-24

  • 分类号G01N232/23;

  • 国家 US

  • 入库时间 2022-08-22 01:03:50

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