A process for the extraction of metal from an ore or concentrate which contains nickel and/or cobalt values and other metals, comprises subjecting the ore or concentrate to acid leaching under pressure at pH=2 to obtain a liquor containing nickel and/or cobalt values, subjecting the liquor to a first precipitation stage at pH of about 5 to 6 to produce a solid containing non nickel and non cobalt metals and a resultant solution containing the nickel and/or cobalt values and subjecting the resultant solution to a second precipitation stage at a pH of about 7 to 8 to produce a solid containing nickel and/or cobalt.
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