首页> 外国专利> The plasticizer energetics comprising a eutectic mixture of bis (2,2 - dinitropropyl) type, 2,2 dinitropropyl - 2,2 - dinitrobutylformal and bis (2,2 - dinitrobutyl) type, and its method of preparation

The plasticizer energetics comprising a eutectic mixture of bis (2,2 - dinitropropyl) type, 2,2 dinitropropyl - 2,2 - dinitrobutylformal and bis (2,2 - dinitrobutyl) type, and its method of preparation

机译:包含双(2,2-二硝基丙基)型,2,2-二硝基丙基-2,2-二硝基丁基甲醛和双(2,2-二硝基丁基)型的低共熔混合物的增塑剂及其制备方法

摘要

The invention relates to an energetic plasticizer consisting of bis (2,2 - dinitropropyl) type, 2, 2 - dinitropropyl - 2, 2 - dinitrobutylformal and of the bis (2, 2 - dinitrobutyl) type in a molar ratio of 20 to 68% / 28 to 50% / 4 to 30% and a process for its preparation, which comprises the dissolution of 2, 2 - dinitropropanol and 2, 2 - dinitrobutanol in an organic solvent to form an organic solution in which the molar ratio of 2, 2 - dinitropropanol at 2, 2 - dinitrobutanol is 3: 1 - 6: 1, the addition to the organic solution of a solution of sulfuric acid, in which a source of formaldehyde has been dissolved, while the temperature of the reaction mixture is maintained at less than 20degrec, and the separation and purification of the product from the reaction mixture.
机译:本发明涉及一种高能增塑剂,其由摩尔比为20至68的双(2,2-二硝基丙基)型,2,2-二硝基丙基-2、2-二硝基丁基甲醛和双(2,2-二硝基丁基)型组成。 %/ 28至50%/ 4至30%及其制备方法,该方法包括将2,2-二硝基丙醇和2,2-二硝基丁醇溶解在有机溶剂中以形成摩尔比为2的有机溶液。在2,2-二硝基丁醇中的2-二硝基丙醇为3:1-6:1,向硫酸溶液中加入已溶解甲醛源的硫酸溶液,而反应混合物的温度为保持低于20℃,并从反应混合物中分离和纯化产物。

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