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Process for making vinyl pyrrolidone/vinyl acetate copolymers having a very low residual vinyl pyrrolidone monomer level within a short production cycle

机译:在短生产周期内制备具有非常低残留乙烯基吡咯烷酮单体含量的乙烯基吡咯烷酮/乙酸乙烯酯共聚物的方法

摘要

Vinyl pyrrolidone/vinyl acetate copolymers having a very low residual vinyl pyrrolidone monomer level, i.e. 100 ppm, preferably only 50 ppm, are made within an advantageously short production cycle, by post-treating an aqueous solution of the copolymer at an elevated temperature of about 120–150° C., preferably about 130° C., under pressure, in the presence of a high temperature initiator, for a period of about 1–4 hours, preferably 2 hours.
机译:通过在较高的温度下对共聚物的水溶液进行后处理,在有利的短生产周期内制得具有非常低的残余乙烯基吡咯烷酮单体含量,即<100ppm,优选仅50ppm的乙烯基吡咯烷酮/乙酸乙烯酯共聚物。在高温引发剂的存在下,在压力下约120-150℃,优选约130℃,持续约1-4小时,优选2小时。

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