This invention, the said method, separation or being at least the aid of 1 kinds of a state where it supports in the method in order to produce under existing of ji -- kurorobisu (-1,5- cyclooctadiene) jiirijiumu of the effective quantity the 3- Kroll's propyl dimethyl Kroll's silane with the hidoroshiriru conversion reaction, the dimethyl hydro Kroll's silane and in the reaction medium which includes allyl chloride as the catalyst, character of ketone, ether, quinone, the anhydride and aromatic possessing and/or at least the C=C double bond 1 and/or the unsaturated hydrocarbon chemical compound (UHC) which at least includes the CC triple bond 1 (hereSo, these unsaturated bond conjugation or can be non conjugation, said UHC is line or annulation (single cyclic type or polycyclic system), it possesses 4 - 30 carbon atoms, the ethylene characteristic 1 - 8 and/or possesses the acetylene characteristic unsaturation, includes the hetero atom 1 or more and as an option) and it adds those which are selected from the group of the chemical compound which consists of those blends to the said reaction medium, but however, when including UHC of 1 kind of kinds or more where the said aid is defined on,These (these) UHC it features that it makes mix at least with the other aid of 1 kinds other than UHC, it is something regarding the production method of the 3- Kroll's propyl dimethyl Kroll's silane.
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