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Process for preparing polymer micro-fibers for solid phase extraction and product obtained.

机译:制备用于固相萃取的聚合物微纤维的方法和获得的产物。

摘要

Process for preparing polymer micro-fibers for solid phase extraction and product obtained.; Process that is used as a capillary mold (1) coated with a polymer, for the protective layer overlying is partially removed by filling the capillary (1) with a polymerization mixture (3) and closing its ends for then introducing the whole in an oven for the time and temperature required for polymerization to occur; then is removed from the oven and broken into several fragments (4) is immersed in a solution (6) with reagents for dissolving the capillary walls, thereby obtaining monolithic polymeric fibers (7) to be employed in solid phase microextraction with ability to retain a compound or family of compounds, which will selectively if the polymerization mixture we add a compound template.
机译:制备用于固相萃取的聚合物微纤维的方法和获得的产物。通过用聚合混合物(3)填充毛细管(1)并封闭其端部,然后将整体引入烤箱中,部分除去覆盖层上用作保护层的毛细管模具(1)的过程。发生聚合反应所需的时间和温度;然后将其从烤箱中取出并分成几个碎片(4),将其浸入溶液(6)中,用试剂溶解毛细管壁,从而获得用于固相微萃取的单块聚合物纤维(7),该纤维能够保留化合物或化合物家族,如果聚合混合物,我们将选择性地添加化合物模板。

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