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2,5-DIAMINOMETHYL-BICYCLO2,2,1HEPTANE AND METHOD FOR PRODUCING THE SAME

机译:2,5-二氨基联苯[2,2,1]庚烷及其制备方法

摘要

PROBLEM TO BE SOLVED: To provide highly pure 2,5-diaminomethyl-bicyclo[2,2,1]heptane substantially free of isomers, and a method for producing the same.;SOLUTION: The 2,5-diaminomethyl-bicyclo[2,2,1]heptane represented by formula (I) or (II) having purity of ≥95% when analyzed by gas chromatography is produced by: protecting amino groups in individual compounds included in an isomer mixture with protective groups; separating the isomers; and deprotecting the protective groups in the separated isomers.;COPYRIGHT: (C)2012,JPO&INPIT
机译:解决的问题:提供基本上不含异构体的高纯度2,5-二氨基甲基-双环[2,2,1]庚烷及其制备方法。解决方案:2,5-二氨基甲基-双环[2通过气相色谱法分析时,纯度为≥95%的由式(I)或(II)表示的1,2,1]庚烷是通过以下方法制备的:通过保护带有保护基的异构体混合物中所包括的各个化合物中的氨基;分离异构体;和分离的异构体中的保护基脱保护。;版权所有:(C)2012,JPO&INPIT

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