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Cleaning apparatus for separating from the mixture DILAKTIDA SUBSTANCES polymerization apparatus, method DILAKTIDA BRANCH OF MIXTURE OF SUBSTANCES AND APPLICATION METHOD AND DEVICE
Cleaning apparatus for separating from the mixture DILAKTIDA SUBSTANCES polymerization apparatus, method DILAKTIDA BRANCH OF MIXTURE OF SUBSTANCES AND APPLICATION METHOD AND DEVICE
FIELD: chemistry.;SUBSTANCE: present invention relates to a method of producing a biodegradable intermolecular cyclic diester of alpha-hydroxycarboxylic acid. The method involves feeding a mixture of materials into a purification apparatus fitted with a column with a dividing wall, dividing the mixture of materials and extracting the purified diester. Said purification apparatus has the following components: a fractionating column, an outlet opening, a mass-exchange cap, a column with a dividing wall which is divided into two zones by a vertical dividing wall, an additional mass-exchange cap, an evaporator and an outlet opening on the collector side. The ratio of the length of the column with a dividing wall to the total length of the purification apparatus range from 0.5 to 0.9.;EFFECT: method enables cheap and efficient separation of diester from mixtures of materials when producing diester with high purity of material and/or optical purity.;19 cl, 9 dwg, 9 ex
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机译:技术领域本发明涉及生产可生物降解的α-羟基羧酸的分子间环状二酯的方法。该方法包括将材料的混合物进料到装配有带有分隔壁的塔的纯化设备中,将材料的混合物分开并提取纯化的二酯。所述纯化装置具有以下组成部分:分馏塔,出口,质量交换帽,具有通过垂直分隔壁被分成两个区域的分隔壁的塔,附加的质量交换帽,蒸发器和集热器侧的出口。具有分隔壁的柱的长度与纯化装置的总长度的比率为0.5到0.9。效果:当生产具有高纯度物料的二酯时,该方法可从物料混合物中廉价有效地分离二酯。 /或光学纯度。; 19 cl,9 dwg,9 ex
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