首页> 外国专利> GRAPHENE PREPARATION METHOD OF HEATING ORGANIC SOLVENT SUSPENSION OF GRAPHITE OXIDE, AND GRAPHENE PREPARED USING SAID METHOD AND APPLICATIONS THEREOF

GRAPHENE PREPARATION METHOD OF HEATING ORGANIC SOLVENT SUSPENSION OF GRAPHITE OXIDE, AND GRAPHENE PREPARED USING SAID METHOD AND APPLICATIONS THEREOF

机译:加热石墨氧化物的有机溶剂悬浮液的石墨烯制备方法及应用所述方法制备的石墨烯及其应用

摘要

Provided is a graphene preparation method of heating an organic solvent suspension of graphite oxide, comprising the following steps: (1) graphite oxide is added to a polar organic solvent, and a suspension is produced by means of ultrasound; (2) the suspension is heated till the suspension is black and partial or complete coagulation occurs; (3) solid-liquid separation is performed on the black suspension obtained in step (2), and a solid is obtained after the polar organic solvent is removed; (4) organic electrolyte solution is dripped onto the solid obtained in step (3), the solid is then suction filtered to obtain a black slurry, and the black slurry is directly coated onto a retainment body; or the solid obtained in step (3) is directly dried to obtain graphene material. Also provided is a graphene prepared using said method, the graphene having a conductivity greater than 1S/m. Also provided are applications of the graphene in super capacitors and lithium ion batteries. The graphene can further be removed of the organic solvent to obtain graphene powder or sheet.
机译:提供一种加热氧化石墨的有机溶剂悬浮液的石墨烯制备方法,其包括以下步骤:(1)将氧化石墨加入极性有机溶剂中,并通过超声制备悬浮液; (2)将悬浮液加热至悬浮液为黑色并发生部分或完全凝结; (3)对步骤(2)中得到的黑色悬浮液进行固液分离,去除极性有机溶剂后得到固体。 (4)将有机电解质溶液滴加到步骤(3)得到的固体上,然后对该固体进行抽滤,得到黑色浆料,将黑色浆料直接涂覆在保持体上;或者将步骤(3)中得到的固体直接干燥得到石墨烯材料。还提供了使用所述方法制备的石墨烯,所述石墨烯具有大于1S / m的电导率。还提供了石墨烯在超级电容器和锂离子电池中的应用。可以进一步从有机溶剂中除去石墨烯以获得石墨烯粉末或片。

著录项

  • 公开/公告号WO2012116594A1

    专利类型

  • 公开/公告日2012-09-07

    原文格式PDF

  • 申请/专利号WO2012CN71069

  • 发明设计人 QU YAN;

    申请日2012-02-13

  • 分类号C01B31/04;H01G9/042;H01M10/052;

  • 国家 WO

  • 入库时间 2022-08-21 17:14:03

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