首页> 外国专利> Synthesizing diamonds, comprises mixing solid, fine carbon of specific modification or several modifications, and optionally with catalyst, pressing the mass into body, sintering, carrying out uniaxial pressing, and cooling sintered body

Synthesizing diamonds, comprises mixing solid, fine carbon of specific modification or several modifications, and optionally with catalyst, pressing the mass into body, sintering, carrying out uniaxial pressing, and cooling sintered body

机译:合成金刚石包括将固体,具有特定修饰或几种修饰的细碳混合,并可选地与催化剂混合,将团块压入物体,烧结,进行单轴压制和冷却烧结体

摘要

Synthesizing diamonds, where solid carbon is exposed to high pressure and high temperature, comprises (i) mixing the solid, fine carbon of specific modification or several modifications with each other, and optionally with catalyst, (ii) pressing the mass into body, and introducing into chamber for field- and pressure-aided sintering processes with pulsed current, (iii) sintering with a current of 1000 A, at a low direct voltage and a pulse rate of millisecond, (iv) carrying out uniaxial pressing, during sintering, (v) cooling sintered body, washing in acid bath then using water, and drying. Synthesizing diamonds, where solid carbon is exposed simultaneously to a high pressure and a high temperature, comprises (i) mixing the solid, fine carbon of a specific modification or several modifications with each other, and optionally with a catalyst, (ii) pressing the mass into a body, and introducing into a chamber for field- and pressure-aided sintering processes with pulsed current, that utilizes on-off controlled direct current supply, (iii) sintering with a current of 1000 A at a low direct voltage and a pulse rate of millisecond, such that the temperature of the body is increased to 1000[deg] C, (iv) simultaneously carrying out uniaxial pressing at 10-100 Mpa, during the sintering under vacuum or protective gas atmosphere, (v) cooling the sintered body for some time, washing in an acid bath then washing using water, and drying in an oven.
机译:合成金刚石,其中将固体碳暴露于高压和高温下,包括(i)将固体,具有特定修饰或几种修饰的细碳彼此相互混合,并可选地与催化剂混合;(ii)将团块压入体内,以及通过脉冲电流将其引入腔室中以进行现场和压力辅助烧结过程;(iii)在低直流电压和毫秒脉冲速率下以1000 A的电流进行烧结;(iv)在烧结过程中进行单轴压制, (v)冷却烧结体,在酸浴中洗涤,然后用水冲洗并干燥。合成金刚石将固体碳同时暴露在高压和高温下,其中包括(i)将固体,具有特定修饰或几种修饰的细碳相互混合,并可选地与催化剂混合,(ii)压制将其质量注入人体,然后引入腔室,以利用脉冲电流控制开闭电流,以脉冲电流进行磁场和压力辅助烧结过程;(iii)以低直流电压和1000 A电流烧结毫秒的脉冲速率,以使主体的温度升高到1000℃,(iv)在真空或保护性气体气氛下烧结期间,同时以10-100 Mpa的压力进行单轴压制。烧结一段时间,先在酸浴中洗涤,然后用水洗涤,然后在烤箱中干燥。

著录项

  • 公开/公告号DE102011014204A1

    专利类型

  • 公开/公告日2012-09-20

    原文格式PDF

  • 申请/专利权人 UNIVERSITAET ROSTOCK;

    申请/专利号DE20111014204

  • 发明设计人 ZHANG FAMING;BURKEL EBERHARD;ROTT GUNNAR;

    申请日2011-03-17

  • 分类号B01J3/08;C01B31/06;

  • 国家 DE

  • 入库时间 2022-08-21 17:04:59

相似文献

  • 专利
  • 外文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号