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Palladium monolithic catalyst on a monolithic support, the method for its preparation and the use of a palladium catalyst on a monolithic support

机译:整体载体上的钯整体催化剂,其制备方法和在整体载体上的钯催化剂的用途

摘要

the subject of the invention is palladowy catalyst for nosniku monolitycznym containing nosnik foil zaroodpornej fecral and affixed to nosnik body active skladajaca with pd and al2o3.with the weight ratio of al2o3 to pd ranges from 1.5 to 3.process for the production of palladium catalyst nosniku monolitycznym request nosnik foil zaroodpornej fecral and naniesionej on nosnik active layer skladajacej with pd and al2o3.with the weight ratio al3o3 to pd is from 1.5 to 3, is thatin the first stage nosnik monolithic film zaroodpornej fecral being modification: odtluszcza in acetone and dried for 2 h at a temperature 105u00b0c,then nosnik giving up digestion in solution of h2so4 of stezeniu 5 - 15% for 2 min at a temperature from 50 - 70u00b0c,after the drought by 4 h at a temperature 105u00b0c and verify to rank wytrawienia nosnika, then in the second stage zol about every game 26,38 - 38,25%.al (oh) 3 of zawartosci 29 - 20% al (oh) 3, respectively, 5%. glycerol and 68,62 - 56,75%.distilled water is mixed with a solution of palladium (ii) zawierajacym 19 - 20% pd to obtain a homogeneous gel and is replaced to sheet composed of active pd and al2o3 with the weight ratio al2o3 to pd ranges from 1.5 to 3, in the third stage naklada on odtluszczony and nosnik etched, after which the drought for 5 h in catalyst temperature of 105 - 120u00b0c and kalcynuje for 35 - 4 h at a temperature of 500 - 550u00b0c.the subject of the invention is also applicable to the palladium catalyst nosniku monolitycznym request nosnik foil zaroodpornej fecral and naniesionej on nosnik active layer skladajasource of pd and al2o3, with the weight ratio of al2o3 to pd ranges from 1.5 to 3 treatment weglowodoru00f3w especially methane by catalytic oxidation.
机译:发明内容本发明的主题是用于nosniku单体的帕拉多维催化剂,其包含nosnik箔zaroodpornej粪便,并以pd和al2o3固定在nosnik身体活性物质skladajaca上,其中al2o3与pd的重量比为1.5至3。 monolitycznym请求在带有pd和al2o3的nosnik活性层skladajacej上使用nosnik箔zaroodpornej粪便和naniesionej。al3o3与pd的重量比为1.5至3,是在第一阶段对nosnik整体膜zaroodpornej粪便进行了改性:odtlacetzc在105 u00b0c的温度下放置2 h,然后nosnik在温度为50 70 u00b0c的温度下干旱4 h后,放弃在5-15%的stezeniu 5-15%的h2so4溶液中消化2分钟。验证对wytrawienia nosnika的排名,然后在第二阶段zol大约每场比赛26,38-38,25%。zawartosci的al(oh)3分别为29-20%al(oh)3 5%。将甘油和68,62-56,75%的蒸馏水与钯(ii)zawierajacym 19-20%pd的溶液混合以获得均匀的凝胶,然后将其替换成由活性pd和al2o3组成的片,重量比为al2o3到pd的范围是1.5到3,在odtluszczony和nosnik蚀刻的第三阶段naklada上,之后在105-120 u00b0c的催化剂温度下干旱5 h,在500-550 的温度下kalcynuje干旱35-4 h本发明的主题也适用于钯催化剂和钯的催化剂上的钯和铝的重量比,铝和钯的重量比为1.5至3。特别是甲烷的催化氧化。

著录项

  • 公开/公告号PL399656A1

    专利类型

  • 公开/公告日2013-04-15

    原文格式PDF

  • 申请/专利权人 POLITECHNIKA WROCLAWSKA;

    申请/专利号PL20120399656

  • 发明设计人 KUCHARCZYK BARBARA;

    申请日2012-06-25

  • 分类号B01J23/89;B01D53/72;B01J37/00;

  • 国家 PL

  • 入库时间 2022-08-21 16:40:13

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