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METHOD OF PRODUCTION OF ELECTROLYTE FOR LITHIUM CHEMICAL CURRENT SOURCES

机译:锂化学电流源电解质的生产方法

摘要

FIELD: electricity.SUBSTANCE: method of production of electrolyte for lithium chemical current sources consists in lithium perchlorate dissolution in propylene carbonate. Lithium perchlorate is loaded into the reactor by weighed portions through certain periods at the temperature of solution 45-60°C. For water distillation in the reactor jacket the heat carrier with the temperature 130-160°C is used, and the pressure in the reactor at the end of the distillation process amounts 1.33-1.6 kPa (10-12 mm Hg) at the mass fraction of water 0.015-0.025%. Lithium perchlorate is loaded into the reactor by three weighed portions, the weight of weighed portions amounts 2.45-2.55 kg, and they are loaded with the interval 12-16 minutes.EFFECT: improvement of quality and stability of composition of the prepared electrolyte for lithium current sources with low water content which allows to improve stability and conservability of the current source up to 25 years without the internal pressure rise.2 cl
机译:领域:电力。物质:用于生产锂化学电流源的电解质的方法包括将高氯酸锂溶解在碳酸亚丙酯中。在45-60℃的溶液温度下,在一定时期内通过称重将高氯酸锂装入反应器中。对于在反应器夹套中进行水蒸馏,使用温度为130-160°C的热载体,蒸馏过程结束时反应器中的压力按质量分数计为1.33-1.6 kPa(10-12 mm Hg)的水量为0.015-0.025%。高氯酸锂通过三个称量部分装入反应器中,称量部分的重量为2.45-2.55 kg,并在12-16分钟的间隔内装入。效果:改善了所制备的锂电解液的质量和组成稳定性水含量低的电流源,可在不增加内部压力的情况下提高电流源的稳定性和可保存性长达25年。2cl

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