preparation of an aqueous solution of a non-crystallizable water-soluble biopolymer or a derivative of said biopolymer at the suitable pH,coating of the substrate with the aqueous solution of the biopolymer prepared in the previous stage by immersion of the substrate in said solution or by using the spin coating technique,conditioning of the aqueous solution of the biopolymer by means of a hydrothermal process consisting of subjecting the coated surface to a flow of nitrogen saturated with water vapor at the temperature of between 100 and 250° C. for a time between 30 minutes and several hours,thermal decomposition of the biopolymer deposited on the substrate in the absence of oxygen at temperatures below 1200° C."/> Method for the preparation of graphene or graphenic materials films on non-metal substrates
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Method for the preparation of graphene or graphenic materials films on non-metal substrates

机译:在非金属基底上制备石墨烯或石墨烯材料膜的方法

摘要

The present invention describes a method for the preparation of graphene or graphenic material films by the carbonization of biopolymers.;The method comprises the following stages:preparation of an aqueous solution of a non-crystallizable water-soluble biopolymer or a derivative of said biopolymer at the suitable pH,coating of the substrate with the aqueous solution of the biopolymer prepared in the previous stage by immersion of the substrate in said solution or by using the spin coating technique,conditioning of the aqueous solution of the biopolymer by means of a hydrothermal process consisting of subjecting the coated surface to a flow of nitrogen saturated with water vapor at the temperature of between 100 and 250° C. for a time between 30 minutes and several hours,thermal decomposition of the biopolymer deposited on the substrate in the absence of oxygen at temperatures below 1200° C.
机译:本发明描述了一种通过生物聚合物碳化制备石墨烯或石墨烯材料薄膜的方法。该方法包括以下步骤: 在合适的pH值下制备不可结晶的水溶性生物聚合物或所述生物聚合物衍生物的水溶液, 通过将前一阶段制备的生物聚合物水溶液浸入基质中,或者通过使用旋涂技术,将其涂覆在基质中, 通过水热过程调节生物聚合物的水溶液,该水热过程包括使涂覆的表面在100至250℃的温度下经受水蒸气饱和的氮气流30分钟至几小时的时间。 , 沉积在基板上的生物聚合物的热分解。在低于1200°C的温度下没有氧气。

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