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LOW-TEMPERATURE NYLON POWDER MATERIAL FOR SELECTIVE LASER SINTERING AND PREPARATION METHOD THEREFOR

机译:选择性激光烧结用低温尼龙粉末材料及其制备方法

摘要

The present invention relates to the technical field of polymer composites, in particular to a low-temperature nylon powder material for selective laser sintering. The low-temperature nylon powder material mainly comprises nylon 12 particles, dodecanedioic acid, double amino-terminated polyethylene glycol, deuterated trifluoroacetic acid, antioxidant, solvent, nucleating agent, plasticizer and silane coupling agent. The low-temperature nylon powder material is prepared by the following steps: uniformly mixing the dodecanedioic acid and nylon 12 particles and putting into a reaction kettle; adding double amino-terminated polyethylene glycol and deuterated trifluoroacetic acid into the reaction kettle; heating and starting stirring to obtain a product; putting the product together with antioxidant, solvent, nucleating agent, plasticizer and silane coupling agent into the reaction kettle, and closing the kettle with a cover; vacuumizing the reaction kettle and introducing nitrogen displacement for protection; starting stirring and reducing the temperature of the kettle body to room temperature; taking out the materials, drying and performing ball milling; and drying the powder to obtain powder with good sphericity and fluidity. The low-temperature nylon powder material provided by the present invention has the characteristics of low preheating temperature, wide preheating window, good aging resistance and adaptability to table boards of various specifications.
机译:本发明涉及聚合物复合材料的技术领域,尤其涉及一种选择性激光烧结的低温尼龙粉末材料。低温尼龙粉末材料主要包括尼龙12颗粒,十二烷二酸,双氨基封端的聚乙二醇,氘代三氟乙酸,抗氧化剂,溶剂,成核剂,增塑剂和硅烷偶联剂。低温尼龙粉料的制备步骤如下:将十二烷二酸与尼龙12颗粒均匀混合后放入反应釜中;向反应釜中加入双氨基末端的聚乙二醇和氘代三氟乙酸。加热并开始搅拌以获得产物;将产物与抗氧化剂,溶剂,成核剂,增塑剂和硅烷偶联剂一起放入反应釜中,并用盖将釜关闭。将反应釜抽真空并引入氮气置换以进行保护;开始搅拌并将釜体的温度降至室温;取出物料,干燥并进行球磨;干燥后得到球形度和流动性好的粉末。本发明提供的低温尼龙粉末材料具有预热温度低,预热窗口宽,耐老化性好,对各种规格的餐桌板具有适应性的特点。

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