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METHOD FOR PRODUCTION OF POTASSIUM HUMATE FROM LOCAL PEATS OF YAMALO-NENETS AUTONOMOUS OKRUG

机译:从亚马洛涅涅茨自治州秋葵本地豆中生产腐植酸钾的方法

摘要

FIELD: agriculture.;SUBSTANCE: invention relates to the field of ecology and soil science. The method for producing potassium humate from local peats of Yamalo-Nenets Autonomous Okrug for reclamation of disturbed and contaminated tundra soils includes: at the first stage - the 0.1 N peat decalcification with sulfuric acid solution at the ratio of 1:20 and its sedimentation; at the second stage - the extraction of humic acids from the resulting sediment 0.1N with sodium hydroxide at the ratio of 1:15, at the third stage - the sedimentation of humic acids with 10% hydrochloric acid solution at the ratio of 50:1, at the fourth stage - the purification of the obtained humic acids sediment by dissolving it in 0.1 N sodium hydroxide solution, adding sodium sulfate solution and 0.1 n hydrochloric acid solution, rinsing with distilled water and drying. At the fifth stage, implemented once, the analysis of the aliphatic, polysaccharide, and aromatic carboxyl carbon content in humic acids is performed by means of the nuclear magnetic resonance spectroscopy 13C-method, by which the regional specificity of a particular peat field is determined, and, using the data obtained, the 2.5% potassium humate solution with pH 7 is subsequently prepared by adding distilled water and 0.1N. solution of potassium hydroxide, and based on express laboratory studies the recommendations are given for its optimal implementation, in particular together with peat for the reclamation of specific plots of disturbed tundra land near the area of peat deposits.;EFFECT: invention provides obtaining chemically pure humic acids, achieving the maximum compliance with environment in the reclamation of disturbed tundra soils.;1 tbl
机译:技术领域本发明涉及生态学和土壤科学领域。由Yamalo-Nenets自治Okrug的本地泥炭生产腐殖酸钾的方法,用于开垦受污染的冻原土壤:第一步:用1:20的硫酸溶液将0.1 N泥炭脱钙并沉降;在第二阶段-用氢氧化钠以1:15的比例从生成的0.1N沉淀物中提取腐殖酸,在第三阶段-用10:50比例的10%盐酸溶液沉淀腐殖酸,在第四阶段-通过将所得腐殖酸沉淀物溶解在0.1 N氢氧化钠溶液中,加入硫酸钠溶液和0.1 n盐酸溶液,用蒸馏水冲洗并干燥来纯化。在第五阶段(实施一次),通过核磁共振波谱 13 C方法对腐植酸中的脂肪族,多糖和芳香族羧基碳含量进行分析,确定特定泥炭田的特异性,并使用获得的数据,随后通过添加蒸馏水和0.1N制备pH为7的2.5%腐植酸钾溶液。氢氧化钾溶液,并根据明确的实验室研究,提供了关于最佳实施的建议,尤其是与泥炭一起用于复垦泥炭沉积区域附近的特定苔原土地的特定土地。腐殖酸,在受干扰的冻原土壤开垦中达到与环境的最大顺应性。1tbl

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