首页> 外国专利> PRODUCTION METHOD FOR ELECTRODE CATALYST, ELECTRODE CATALYST, COMPOSITION FOR FORMING GAS DIFFUSION ELECTRODE, GAS DIFFUSION ELECTRODE, MEMBRANE-ELECTRODE ASSEMBLY (MEA), AND FUEL CELL STACK

PRODUCTION METHOD FOR ELECTRODE CATALYST, ELECTRODE CATALYST, COMPOSITION FOR FORMING GAS DIFFUSION ELECTRODE, GAS DIFFUSION ELECTRODE, MEMBRANE-ELECTRODE ASSEMBLY (MEA), AND FUEL CELL STACK

机译:电极催化剂的生产方法,电极催化剂,形成气体扩散电极的成分,气体扩散电极,膜电极组件(MEA)和燃料电池堆

摘要

Provided is a production method of an electrode catalyst that can reduce the content of chlorine species reliably and sufficiently through a simple operation, even when using an electrode catalyst precursor containing a high concentration of chlorine (Cl) species as a raw material of the electrode catalyst. The production method of the electrode catalyst has a core-shell structure including a core part formed on a support and a shell part formed to cover at least a part of a surface of the core part. The production method includes a first step (1) of preparing a first liquid with an electrode catalyst precursor (I) being dispersed in ultrapure water by adding the electrode catalyst precursor (I) to the ultrapure water, the electrode catalyst precursor (I) being produced using a material containing chlorine (Cl) species, and exhibiting a chlorine (Cl) species concentration not lower than a first chlorine (Cl) species concentration when measured by X-ray fluorescence (XRF) spectroscopy; and a second step (2) of preparing a second liquid by dispersing an electrode catalyst precursor (II), the electrode catalyst precursor (II) being obtained by filtrating and washing the electrode catalyst precursor (I) contained in the first liquid with ultrapure water , and then performing washing until an electric conductivity p of a filtrate has become a first value or lower.
机译:提供一种电极催化剂的制造方法,即使使用含有高浓度氯(Cl)物种的电极催化剂前体作为电极催化剂的原料,也可以通过简单的操作可靠且充分地减少氯物种的含量。 。电极催化剂的生产方法具有核-壳结构,其包括形成在载体上的核部分和形成为覆盖核部分的至少一部分表面的壳部分。该生产方法包括第一步骤(1):通过将电极催化剂前体(I)添加到超纯水中来制备第一液体,其中将电极催化剂前体(I)分散在超纯水中。使用含有氯(Cl)物质的材料生产,并且当通过X射线荧光(XRF)光谱法测量时,显示出不低于第一氯(Cl)物质浓度的氯(Cl)物质浓度;第二步(2)是通过分散电极催化剂前体(II)来制备第二液体的,该电极催化剂前体(II)是通过用超纯水过滤和洗涤包含在第一液体中的电极催化剂前体(I)而获得的。然后进行洗涤,直到滤液的电导率p达到第一值或更低。

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