首页> 外国专利> METHOD FOR PREPARING LITHIUM IRON PHOSPHATE MATERIAL COATED WITH CARBON NANORIBBON

METHOD FOR PREPARING LITHIUM IRON PHOSPHATE MATERIAL COATED WITH CARBON NANORIBBON

机译:碳纳米管包覆磷酸铁锂材料的制备方法

摘要

The present application provides a method for preparing a lithium iron phosphate material coated with carbon nanoribbon, including the steps of: 1) fully and uniformly dispersing carbon nanoribbons in an aqueous solution by means of stirring and ultrasonic dispersion, and obtaining a mixture; 2) adding a lithium source, an iron source and a phosphorous source at a molar ratio of Li:Fe:P=1:1:1 into the mixture of step 1) under the protection of inert gas, adding water and stirring to form a slurry, and refluxing the slurry; 3) washing and drying the slurry to obtain a primary lithium iron phosphate material coated with carbon nanoribbon; and 4) annealing the primary lithium iron phosphate material coated with carbon nanoribbon of step 3) at high-temperature in a protective atmosphere of argon containing 5-10% v/v of hydrogen, and obtaining the lithium iron phosphate material coated with carbon nanoribbon.
机译:本申请提供了一种制备碳纳米带包覆的磷酸锂铁材料的方法,包括以下步骤:1)通过搅拌和超声分散将碳纳米带充分均匀地分散在水溶液中,得到混合物; 2)在惰性气体保护下,将锂,铁,磷以Li:Fe:P = 1:1:1的摩尔比加入步骤1)的混合物中,加水搅拌形成浆料,并使浆料回流; 3)洗涤并干燥浆料,得到碳纳米带包覆的磷酸铁锂初材料。 4)在含有5-10%v / v氢的氩气的保护气氛中,在高温下对步骤3)的碳纳米带包覆的一次磷酸锂铁材料进行退火,得到碳纳米带包覆的磷酸锂铁材料。 。

著录项

  • 公开/公告号US2018102530A1

    专利类型

  • 公开/公告日2018-04-12

    原文格式PDF

  • 申请/专利权人 OPTIMUM BATTERY CO. LTD.;

    申请/专利号US201715730759

  • 发明设计人 GUOLONG YANG;HAITAO WANG;

    申请日2017-10-12

  • 分类号H01M4/04;H01M10/0525;H01M4/1397;H01M4/36;H01M4/58;H01M4/587;

  • 国家 US

  • 入库时间 2022-08-21 13:05:38

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