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Titanium-dioxide-based double-layer hollow material, preparation method thereof, and application thereof in photocatalytic treatment of hydrogen sulfide

机译:二氧化钛基双层中空材料,其制备方法及其在硫化氢的光催化处理中的应用

摘要

A preparation method of a titanium-dioxide-based double-layer hollow material includes the following steps: (1) using polystyrene nanospheres with particle size of 180 nm as a template, tetrabutyl titanate as a precursor, to prepare hollow titanium dioxide by calcining; (2) subjecting said hollow titanium dioxide to carboxylation modification to prepare carboxylated titanium dioxide; and (3) dispersing said carboxylated titanium dioxide in ethanol, using chromic nitrate nonahydrate as an assembly agent and trimesic acid as a crosslinking agent to carry out layer-by-layer self-assembly so as to prepare the titanium-dioxide-based double-layer hollow material.
机译:二氧化钛类双层中空材料的制备方法包括以下步骤:(1)以粒径为180nm的聚苯乙烯纳米球为模板,钛酸四丁酯为前体,通过煅烧制备中空二氧化钛。 (2)对所述空心二氧化钛进行羧化改性,制备羧化二氧化钛。 (3)将所述羧化二氧化钛分散在乙醇中,以硝酸无水铬酸水为组装剂,以偏苯三酸为交联剂进行层层自组装,制备二氧化钛基双层空心材料。

著录项

  • 公开/公告号US10160659B2

    专利类型

  • 公开/公告日2018-12-25

    原文格式PDF

  • 申请/专利权人 SOOCHOW UNIVERSITY;

    申请/专利号US201715853906

  • 发明设计人 JIANMEI LU;DONGYUN CHEN;JUN JIANG;

    申请日2017-12-25

  • 分类号C01G23/053;C01G23/08;C08L25/06;C08J7/12;B01J35;B01D53/52;B05D1/18;B05D7;C01B17/16;B29B11/14;C08K3/22;

  • 国家 US

  • 入库时间 2022-08-21 12:13:24

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