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PREPARATION METHOD OF FUNCTIONALIZED GRAPHENE WITH GAS SENSITIVITY AND GAS-SENSITIVE INK

机译:具有气敏性和气敏性油墨的功能性石墨烯的制备方法

摘要

#$%^&*AU2020102360A420201105.pdf#####Abstract The present application discloses a preparation method of a functionalized graphene with gas sensitivity and a gas-sensitive ink, wherein the preparation method includes the following steps: preparing a sulfonated graphene oxide; and taking potassium stannate as a tin source, 1-cysteine as a sulfur source, CTAB as a dispersing agent, and crystallizing tin sulfide crystals on surfaces of the functionalized graphene under a hydrothermal condition to form a functionalized graphene gas-sensitive material loaded with the tin sulfide. The functionalized graphene obtained by adopting the technical solution of the present application has better dispersion performance in a solvent, and the obtained gas-sensitive ink can rapidly adsorb nitrogen dioxide and ammonia gas molecules, and has extremely high sensitivity, without being influenced by an external humidity environment; and the ink can be directly written on common substrates such as glass, paper, cloth without participation of an interdigital electrode. The preparation method is rapid, simple, convenient, repeatable and easy to control.Drawings - SnS S-rGO 90. -SnS rGO 8070 40 o s530 20 100 500 1000 1500 2000 2500 3000 3500 4000 Time (s) FIG. 1 0-50 g - SnSWS-rGO -20- - SnS2/rGO 1000 2000 3000 4000 5000 6000 Time (s) FIG. 2
机译:#$%^&* AU2020102360A420201105.pdf #####抽象本申请公开了一种用气体制备功能化石墨烯的方法敏和气敏油墨,其中所述制备方法包括以下步骤:制备磺化氧化石墨烯;以锡酸钾为锡源,以1-半胱氨酸为锡源硫源,CTAB作为分散剂,使硫化锡晶体在在水热条件下官能化的石墨烯形成官能化的石墨烯装有硫化锡的气体敏感材料。通过以下方法获得的功能化石墨烯采用本发明的技术方案,具有较好的分散性能。溶剂,所得的气敏油墨可快速吸附二氧化氮和氨气分子,并具有极高的灵敏度,不受外界湿度的影响环境;墨水可以直接写在玻璃,纸,布等普通基材上没有叉指电极的参与。制备方法快速,简便,方便,可重复且易于控制。图纸-SnS S-rGO90. -SnS rGO807040o s53020100 500 1000 1500 2000 2500 3000 3500 4000时间(秒)图。 1个0-50G-SnSWS-rGO-20--SnS2 / rGO1000 2000 3000 4000 5000 6000时间(秒)图。 2

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