Nd-Fe-B/α-Fe multi-layered thick film-magnets were synthesized by PLD method from a Nd2.4Fe14B/α-Fe composite target. In order to improve magnetic properties and their reproducibility, effects of the stacking period of Nd-Fe-B/α-Fe layers, tp, the target-substrate distance, DTS, and the laser beam energy on a target, EL, on them were studied. The reproducibility of magnetic properties was improved significantly by decreasing LE. In particular, the standard deviation of the Nd content was suppressed within 3%, when LE was reduced from a value higher than 200 mJ/mm2 to 25 mJ/mm2. An increase in DTS and selection of a suitable tp value improved the maximum energy product (BH)max. The largest (BH)max value obtained in this investigation was 112 kJ/m3, which is higher than the values reported previously for isotropic film-magnets thicker than 10 μm. Origins of superior magnetic properties were discussed from the viewpoints of suitable interlayer exchange interaction between Nd-Fe-B and α-Fe layers and morphology of prepared film-magnets.
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机译:采用PLD法由Nd2.4Fe14B /α-Fe复合靶材合成了Nd-Fe-B /α-Fe多层厚膜磁体。为了改善磁性能及其可重复性,Nd-Fe-B /α-Fe层的堆叠时间tp,靶-基片距离DTS以及靶上EL上的激光束能量的影响被研究了。降低LE可以显着提高磁性能的可重复性。特别地,当LE从高于200mJ / mm 2的值减小到25mJ / mm 2时,Nd含量的标准偏差被抑制在3%以内。 DTS的增加和适当tp值的选择改善了最大能量积(BH)max。在这项研究中获得的最大(BH)max值为112 kJ / m3,高于先前报道的厚度大于10μm的各向同性薄膜磁铁的值。从Nd-Fe-B和α-Fe层之间适当的层间交换相互作用以及制得的薄膜磁体的形态的角度,讨论了优异的磁性质的起源。
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