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Diastereoselective Synthesis of Novel Heterocyclic Scaffolds through Tandem Petasis 3-Component/Intramolecular Diels-Alder and ROM-RCM Reactions

机译：通过串联petasis 3组分/分子内Diels-alder和ROm-RCm反应非对映选择性合成新型杂环支架

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摘要

A high-yielding, stereoselective and extraordinarily complexity generatingPetasis 3-component/intramolecular Diels-Alderreaction has been developed. In combination with ROM-RCM, rapid access to complex sp-rich heterocyclic scaffolds amenableto subsequent functionalization and library synthesis is provided.

机译：已经开发了产生高产，立体选择性和异常复杂的Petasis 3组分/分子间狄尔斯-阿尔德反应的产品。与ROM-RCM结合使用，可以快速访问适合后续功能化和库合成的富含sp的复杂杂环骨架。

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Ishøy Mette; Petersen Rico; Petersen Michael Åxman; Wu Peng; Clausen Mads Hartvig; Nielsen Thomas Eiland;
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年度 2018
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专利

1. Generation of a Heteropolycyclic and sp~3-Rich Scaffold for Library Synthesis from a Highly Diastereoselective Petasis/ Diels-Alder and ROM-RCM Reaction Sequence [J] . Thomas Flagstad, Carlos M.G.Azevedo, Nikolaj S.Troelsen, European journal of organic chemistry . 2019,第5期

机译：从高度映选择性的Petasis / Diels-Alder和ROM-RCM反应序列中产生杂多环和SP〜3富型脚手库的富含型富脚的支架
2. Diastereoselective synthesis of bridged polycyclic alkaloids via tandem acylation/intramolecular diels-alder reaction [J] . Chen C.-H., Yellol G.S., Tsai C.-H., The Journal of Organic Chemistry . 2013,第19期

机译：通过串联酰化/分子间狄尔斯-阿尔德反应的非对映选择性合成桥联多环生物碱
3. Petasis three-component reactions for the synthesis of diverse heterocyclic scaffolds [J] . Peng Wu, Thomas E. Nielsen Drug discovery today. Technologies . 2018,第期

机译：用于合成各种杂环支架的唾液三分反应
4. Tandem Diels-Alder Reactions of Arynes: New Method for the Synthesis of Large Poly cyclic Aromatic Compounds and Nanographenes [C] . Diego Pena, Alejandro Criado, Dolores Perez European Symposium on Organic Chemistry . 2009

机译：Arynes的串联Diels-Alder反应：用于合成大聚环芳族化合物和纳米的新方法
5. I. Studies toward the formal synthesis of (+)-aldosterone. II. Type 2 intramolecular hetero Diels-Alder reaction and the discovery of a novel tandem hetero Diels-Alder reaction. [D] . Bear, Brian Richard. 2001

机译：I.对（+）-醛固酮的形式合成的研究。二。 2型分子内杂Diels-Alder反应和新型串联杂Diels-Alder反应的发现。
6. Diastereoselective Synthesisof Highly SubstitutedTetrahydrofurans by Pd-Catalyzed Tandem Oxidative Cyclization–RedoxRelay Reactions Controlled by Intramolecular Hydrogen Bonding [O] . JoshuaL. Brooks, Liping Xu, Olaf Wiest, -1

机译：非对映选择性合成高度替代钯催化串联氧化环化氧化还原四氢呋喃分子内氢键控制的接力反应
7. Chiral Template Mediated Diastereoselective Intramolecular Diels-Alder Reaction Using Furan as a Diene. Toward the Synthesis of Enantiopure Trisubstituted Tetrahydroepoxyisoindolones [O] . -1

机译：手性模板介导使用呋喃作为二烯的异映选择性分子内二极管 - Alder反应。朝向对映的合成映三羟基苯并苯并二异吲哚酮
8. Pressure-Induced Diastereoselectivity in Photoinduced Diels-Alder Reactions. [R] . Chung, W. S., Turro, N. J. 1989

机译：光诱导Diels-alder反应中的压力诱导非对映选择性。

Diastereoselective Synthesis of Novel Heterocyclic Scaffolds through Tandem Petasis 3-Component/Intramolecular Diels-Alder and ROM-RCM Reactions

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