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Potato extract as reducing agent and stabiliser in a facile green one-step synthesis of ZnO nanoparticles

机译:马铃薯提取物作为还原剂和稳定剂,易于绿色一步法合成ZnO纳米粒子

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摘要

A facile green recipe was developed to synthesise highly pure, safe and durable zinc oxide nanoparticles (ZnO Nps) using homemade starch-rich potato extract. The ZnO Nps were synthesised using zinc nitrate and potato extract, and the whole reaction is carried out for 30 min at 80 °C. In the synthesis, starch-rich potato extract acted as the reducing agent and as a stabilising layer on freshly formed ZnO Nps. Hexagonal (wurtzite) shaped ZnO Nps with size about 20 ± 1.2 nm were synthesised and characterised using X-ray diffraction, transition electron microscope and scanning microscopy analyses. Fourier transform infrared spectral analysis indicated that highly pure ZnO nanopowders were obtained at higher temperatures. The use of environmentally benign and renewable material as the respective reducing and protecting agents, starch-rich potato extract, as well as a gentle solvent medium (H2O), offered a simple and quite efficient procedure for the synthesis of ZnO Nps in neutral medium with promising potential for biological and biomedical applications.
机译:开发了一种简便的绿色配方,可以使用自制的富含淀粉的马铃薯提取物来合成高纯度,安全和耐用的氧化锌纳米颗粒(ZnO Nps)。 ZnO Nps用硝酸锌和马铃薯提取物合成,整个反应在80°C下进行30分钟。在合成过程中,富含淀粉的马铃薯提取物在新鲜形成的ZnO Nps上充当还原剂和稳定层。合成了尺寸约为20±1.2 nm的六方(纤锌矿)形ZnO Nps,并使用X射线衍射,过渡电子显微镜和扫描显微镜分析对其进行了表征。傅立叶变换红外光谱分析表明,在较高温度下可获得高纯度的ZnO纳米粉。使用环境友好的可再生材料作为各自的还原剂和保护剂,富含淀粉的马铃薯提取物以及温和的溶剂介质(H2O),为在中性介质中使用ZnO Nps合成提供了一种简单而高效的方法,在生物和生物医学方面的应用前景广阔。

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