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Annealing Temperature Effect on Structural and Magnetic Properties of Nano Crystalline Ni0.6Co0.2Cu0.2Fe2O4 (NCCFO) Thin Filmud

机译:退火温度对纳米晶Ni0.6Co0.2Cu0.2Fe2O4(NCCFO)薄膜结构和磁性的影响

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摘要

In the present work we prepared NCCFO thin films by metallo-organic decomposition (MOD) technique and studied the effect of different annealing temperature on structural and magnetic properties. The prepared thin film samples are annealed at four different temperatures (550 degrees C, 650 degrees C, 750 degrees C, 850 degrees C) for two hours. The XRD results confirmed the cubic spinel structure at different temperature with the sharpening of (311) peaks. The crystallite size was found to increase with annealing temperature and was further confirmed from AFM images. All samples show distinct hysteresis curves and improved ferromagnetic properties. The saturation magnetization increases with increase in annealing temperatures, while coercivity shows anomalous behavior which could be due to transformation from single to multi domain system. The ferrite thin films with distinct magnetic properties can find applications in many technological advanced nano devices.ud
机译:在本工作中,我们通过金属有机分解(MOD)技术制备了NCCFO薄膜,并研究了不同退火温度对结构和磁性能的影响。所制备的薄膜样品在四个不同的温度(550摄氏度,650摄氏度,750摄氏度,850摄氏度)下退火两个小时。 XRD结果证实了在不同温度下立方尖晶石结构随着(311)峰的锐化。发现微晶尺寸随退火温度而增加,并且从AFM图像进一步证实。所有样品均显示出明显的磁滞曲线和改善的铁磁性能。饱和磁化强度随退火温度的升高而增加,而矫顽力则表现出异常行为,这可能是由于从单畴系统向多畴系统的转变。具有独特磁性的铁氧体薄膜可以在许多技术先进的纳米器件中找到应用。 ud

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