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Synthesis and Characterization of La0.8Sr0.2Ga0.8Mg0.2O3-δ Nano-Particle by Aerosol Plasma Pyrolysis

机译:气溶胶等离子体热解法合成La0.8sr0.2Ga0.8mg0.2O3-δ纳米粒子及其表征

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摘要

Spherical La0.8Sr0.2Ga0.8Mg0.2O3-δ (LSGM) precursor powders were synthesized by aerosol plasma pyrolysis using an aqueous solution of metal nitrate. As-prepared powders obtained by this method were found to have a spherical morphology with a bimodal size distribution of nanosized (primary) and submicron-sized (secondary) particles. The average size of the primary particles was less than 100 nm. X-ray diffraction (XRD) patterns showed that as-prepared powders crystallized to LSGM and other phases. XRD revealed that LSGM pellets were crystallized to a perovskite structure after sintering at 1300 °C for 10 h.
机译:使用金属硝酸盐水溶液通过气溶胶等离子体热解合成球形La0.8Sr0.2Ga0.8Mg0.2O3-δ(LSGM)前体粉末。发现通过该方法获得的制备的粉末具有球形形态,具有纳米级(初级)和亚微米级(次级)颗粒的双峰尺寸分布。一次颗粒的平均尺寸小于100nm。 X射线衍射(XRD)图谱显示所制备的粉末结晶为LSGM和其他相。 XRD显示,在1300℃下烧结10小时后,LSGM粒料结晶成钙钛矿结构。

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