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Synthesis and characterization of zeolite NaP using kaolin waste as a source of silicon and aluminum.

机译:高岭土废料作为硅和铝源的合成和表征Nap分子筛。

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摘要

The synthesis of zeolite NaP using kaolin waste, from the Amazon region, as a predominant source of silicon and aluminum has been studied. The zeolitisation process occurred in hydrothermal conditions using static autoclaving and the effects of time, temperature, and the Si/Al ratio were investigated. The starting material and the phases formed as reaction products were characterized by XRD, SEM and FTIR. The results showed that pure zeolite NaP is hydrothermally synthesized, at 100 °C for 20 hours, using metakaolin waste material in alkaline medium in presence of additional silica. The XRD and SEM analyses indicate that the synthesized zeolite presents good crystallinity
机译:已经研究了使用亚马逊河地区的高岭土废料作为硅和铝的主要来源合成NaP沸石的方法。在静态热压作用下,水热条件下发生了沸石化过程,研究了时间,温度和Si / Al比的影响。通过XRD,SEM和FTIR表征了原料和作为反应产物形成的相。结果表明,使用偏高岭土废料在碱性介质中,在附加的二氧化硅的存在下,于100°C水热合成了纯NaP沸石。 XRD和SEM分析表明,合成沸石具有良好的结晶度。

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