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Strain softening and microstructural evolution of anorthite aggregates and quartz-anorthite layered composites deformed in torsion

机译:钙长石聚集体和石英 - 钙长石复合材料的应变软化和微观结构演变在扭转中变形

摘要

Torsion experiments of anorthite (An) aggregates and layered composites with equal volume fractions of quartz (Qtz) and An were performed in a gas-medium apparatus at a confining pressure of 400 MPa, temperatures from 1373 to 1473 K, and twist rates from 1.0 x 10(-4) to 3.0 x 10(-4) rad/s. Dense specimens were fabricated from An glass and Qtz crystalline powder using hot isostatic pressing (HIP) techniques. Both An aggregates and Qtz-An layered composites show a continuous strain weakening from a peak stress at gamma=0.2-0.3 to gamma=3.2, and steady-state flow has not reached under the experimental conditions. The weakening is even more pronounced in the layered composites than the monolithic aggregates, suggesting channeling or localization of flow into the weak material between strong layers. The sheared An specimens developed pervasively C-S-C' structures which are similar to those observed in natural ductile shear zones. TEM and electron backscattering diffraction (EBSD) fabric analyses suggest that grain boundary migration recrystallization-accommodated dislocation creep with (010)[100] as the dominant slip system was operating in the An. The strain softening may be due to the development of crystallographic preferred orientation (CPO), the operation of dynamic recrystallization and the formation of extremely fine-grained recrystallized material in the narrow C' shear bands. (C) 2004 Elsevier B.V All rights reserved.
机译:在气体介质装置中,在400 MPa的围压,1373至1473 K的温度和1.0的扭曲速率下,在气体介质设备中进行了钙锰矿(An)聚集体和具有相等体积分数的石英(Qtz)的层状复合材料的扭转实验。 x 10(-4)至3.0 x 10(-4)rad / s。使用热等静压(HIP)技术由玻璃和Qtz结晶粉末制成致密的样品。 An聚集体和Qtz-An层状复合材料均显示出连续的应变,从γ= 0.2-0.3的峰值应力减弱到γ= 3.2,并且在实验条件下未达到稳态流动。在层状复合材料中,这种弱化甚至比整体聚集体更为明显,这表明在强层之间,流向弱材料的通道化或局部化。剪切的An样品普遍形成了C-S-C'结构,类似于在天然延性剪切带中观察到的结构。 TEM和电子反向散射衍射(EBSD)织物分析表明,以(010)[100]为主要滑移系统的晶界迁移再结晶适应位错蠕变在An中运行。应变软化可能是由于结晶学优选取向(CPO)的发展,动态重结晶的操作以及在狭窄的C'剪切带中形成了极细晶粒的重结晶材料所致。 (C)2004 Elsevier B.V保留所有权利。

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