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Cyclic nanoindentation studies on TiN and Ti-TiN multilayer coatings deposited on Zr-based metallic glasses

机译:Zr基金属玻璃沉积TiN和Ti-TiN多层涂层的循环纳米压痕研究

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摘要

Cyclic nanoindentation tests were carried out to investigate the influence of TiN and Ti-TiN multilayer coatings on the mechanical properties of Zr-based metallic glass. TiN and Ti-TiN multilayer coatings have been deposited on Zr60Ni10Cu20Al10 metallic glass substrate by RF sputtering. The deposition process was done at room temperature under nitrogen reactive gas using metallic titanium target. The two deposited coating have a thickness of 300 nm. Several cyclic nanoindentation measurements were conducted on TiN, Ti-TiN coatings deposited on Zr-based metallic glass samples at various loading rates. We have found that the coated metallic samples shows higher mechanical properties such as hardness and reduced elastic modulus compared to the bulk metallic glass substrate. Furthermore, the designed experiments shows a difference in the deformation behaviour of the samples, as being analysed through the obtained load-displacement curves with the AFM pictures of the residual indentation imprints. The effect of the loading rate on the deformation behaviours of these samples was also discussed in this work.
机译:进行了循环纳米压痕测试,以研究TiN和Ti-TiN多层涂层对Zr基金属玻璃机械性能的影响。 TiN和Ti-TiN多层涂层已通过RF溅射沉积在Zr60Ni10Cu20Al10金属玻璃基板上。使用金属钛靶在室温下在氮气反应气体下完成沉积过程。两次沉积的涂层的厚度为300 nm。在以不同加载速率沉积在Zr基金属玻璃样品上的TiN,Ti-TiN涂层上进行了几次循环纳米压痕测量。我们已经发现,与块状金属玻璃基底相比,涂覆的金属样品显示出更高的机械性能,例如硬度和降低的弹性模量。此外,设计的实验表明,样品的变形行为有所不同,这是通过使用残留压痕印记的AFM图片通过获得的载荷-位移曲线进行分析而得出的。这项工作中还讨论了加载速率对这些样品的变形行为的影响。

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