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Electron microscpy study of deformation and recrystallization behavior of pure tin for mitigation of whiskers

机译:电子显微镜研究纯锡的变形和再结晶行为,以减轻晶须

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摘要

The clarification of whisker growth mechanism is a key to the mitigation of tin-whiskers. In order to confirm the growth model the present authors had proposed, the process of recrystallization of tin was investigated. A single crystal of tin was prepared by using a slow-cooling method and plate samples were prepared by using a spark-cutter and electro-polishing. Deformation was applied to the plate samples by scratching. The microstructural changes with time at room temperature after scratching were observed by scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD). The experimental results showed clearly that recrystallization can proceed even at room temperature. A tensile test was also performed in order to investigate its ordinary deformation behavior. The present results have supported the model for tin whisker growth mechanism, suggesting that if the recrystallization phenomenon can be controlled to proceed homogenously in tin solder and plating, the whisker growth will be mitigated.
机译:晶须生长机理的阐明是缓解锡须的关键。为了确定作者提出的生长模型,研究了锡的重结晶过程。使用缓慢冷却法制备锡单晶,并使用火花切割机和电抛光法制备板样品。通过刮擦将变形施加到板样品上。通过扫描电子显微镜(SEM)和电子背散射衍射(EBSD)观察到划痕后室温下随时间的显微组织变化。实验结果清楚地表明,即使在室温下也可以进行重结晶。为了研究其正常的变形行为,还进行了拉伸试验。目前的结果支持了锡晶须生长机理的模型,表明如果可以控制再结晶现象在锡焊料和电镀中均匀地进行,则晶须生长将得到缓解。

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