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Optimization of gold and silver nanoparticles production by laser ablation in deionized water

机译:在去离子水中激光烧蚀优化金和银纳米颗粒的生产

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摘要

Colloidal solutions of gold and silver nanoparticles (NPs) were synthesized using a Q-switched Nd:YAG laser (1064 nm, 6 ns, 1 Hz ) ablation. Gold and silver bars were immersed in deionized water and irradiated by laser pulses for 4 min. The laser fluence was verified within the range of 21 – 39 J/cm2 with a fixed beam diameter of 1.6 mm. The effect of laser pulse fluence on both size and ablation efficiency of gold and silver nanoparticles were studied. The optical spectral characterization and morphological analysis of these nanoparticles were carried out by UV-Vis spectrophotometer and transmission electron microscopy (TEM), respectively. The average particle size for Au and Ag are 38.0 ± 10.3 nm and 31.3 ± 10.5 nm at corresponding optimized laser fluence of 31 and 25 Jcm-2 respectively.
机译:金和银纳米粒子(NPs)的胶体溶液使用Q开关Nd:YAG激光(1064 nm,6 ns,1 Hz)烧蚀合成。将金条和银条浸入去离子水中,并用激光脉冲照射4分钟。在固定光束直径为1.6 mm的情况下,验证了激光通量在21 – 39 J / cm2的范围内。研究了激光脉冲能量密度对金和银纳米颗粒的尺寸和烧蚀效率的影响。这些纳米颗粒的光谱特征和形态分析分别通过紫外可见分光光度计和透射电子显微镜(TEM)进行。在相应的优化激光通量分别为31和25 Jcm-2时,Au和Ag的平均粒径分别为38.0±10.3 nm和31.3±10.5 nm。

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