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Surface characterization of thin titania films prepared at low temperatures

机译:低温制备的二氧化钛薄膜的表面表征

摘要

Nanostructured thin films of titanium dioxide were produced on cotton, glass and silicon substrates from alkoxide solutions at low temperatures. The microstructure and elemental composition of these films were investigated by scanning electron microscopy (SEM) and energy dispersive X-ray microanalysis (EDX), respectively. The crystallinity of the films was studied by transmission electron microscopy (TEM) and Raman spectroscopy. The UV absorption of titania-coated cotton substrates was also studied. The leaching stability of the titania films coated on cotton after washing reveals a high level of adhesion which might be attributable to a dehydration reaction between titania and the cellulosic hydroxyl groups of cotton.
机译:在低温下,从醇盐溶液在棉,玻璃和硅基板上生产出纳米结构的二氧化钛薄膜。通过扫描电子显微镜(SEM)和能量色散X射线显微分析(EDX)分别研究了这些薄膜的微观结构和元素组成。通过透射电子显微镜(TEM)和拉曼光谱研究膜的结晶度。还研究了涂覆二氧化钛的棉基材的紫外线吸收。洗涤后涂覆在棉花上的二氧化钛薄膜的浸出稳定性显示出高水平的粘附力,这可能归因于二氧化钛与棉花纤维素羟基之间的脱水反应。

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