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Porous FeAl intermetallics fabricated by elemental powder reactive synthesis

机译:元素粉末反应合成制备多孔FeAl金属间化合物

摘要

Fabrication of porous FeAl intermetallics has been realized through the Fe and Al elemental powder reactive synthesis. The swelling behavior, synthesis process and microstructure of the porous FeAl intermetallics fabricated by reactive synthesis have been systematically studied. The pore structural parameters as a function of the sintering temperature have also been systematically investigated. It has been confirmed that the pore evolution in the porous FeAl intermetallics is attributed to the following four steps: the inter-particle pores formed during the pressing procedure, the Kirkendall pores formed during the solid-state sintering, pore formed through the liquid Al reaction, and the phase transformation during the high temperature sintering.
机译:通过Fe和Al元素粉末反应性合成已经实现了多孔FeAl金属间化合物的制备。对反应合成法制备的多孔FeAl金属间化合物的溶胀行为,合成过程和微观结构进行了系统研究。还已经系统地研究了孔结构参数随烧结温度的变化。已经证实,多孔FeAl金属间化合物的孔演化归因于以下四个步骤:压制过程中形成的颗粒间孔,固态烧结过程中形成的Kirkendall孔,液态Al反应形成的孔,以及高温烧结过程中的相变。

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