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Illumination effects in holographic imaging of the electrostatic potential of defects and pn-junctions in transmission electron microscopy

机译:全息图成像中透射电子显微镜中缺陷和pn结的静电势的照明效应

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摘要

Off-axis holography has successfully revealed the built-in potential in highly doped pn-junctions, making holographic phase retrieval in transmission electron microscopy (TEM) a prospective tool for imaging the electrostatic potential in a semiconductor sample or device. The effect of electron-hole pair generation during electron illumination and the presence of defect rich amorphized sample surfaces in a TEM sample on the electrostatic potential is investigated for the test case of an electrically active grain boundary and a pn-junction in silicon by numerical simulation. In the case of the grain boundary, the pair generation in the electron beam leads to significantly increased recombination currents into trap state defects. As a result, the trapped charge in the defects is decreased and the potential drop around the electrically active defect is considerably reduced, for electron-hole pair generation rates typically present in a TEM experiment even below the detection limit of holography. In the case of pn-junctions distorted potential maps are predicted for dopant densities smaller than 10(17) cm(-3).
机译:离轴全息术已成功揭示了高掺杂pn结中的内在电势,从而使透射电子显微镜(TEM)中的全息相检索成为对半导体样品或器件中的电势进行成像的前途工具。通过数值模拟研究了电活性晶界和硅中pn结的测试情况,研究了电子照射过程中电子-空穴对的产生以及TEM样品中存在缺陷的非晶化样品表面对静电势的影响。 。在晶界的情况下,电子束中对的产生导致复合电流显着增加,成为陷阱态缺陷。结果,对于TEM实验中通常存在的电子-空穴对生成速率,甚至低于全息图的检测极限,缺陷中的俘获电荷减少,并且电活性缺陷周围的电势降大大降低。在pn结的情况下,对于小于10(17)cm(-3)的掺杂剂密度,可能会扭曲电势图。

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