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Supercritical fluid extraction of corn germ oil: Study of the influence of process parameters on the extraction yield and oil quality

机译:玉米胚芽油的超临界萃取:工艺参数对萃取得率和油品质的影响

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摘要

The supercritical fluid extraction of corn germ oil has been studied in this work. Extractions were carriedudout at different pressure, temperature and flow rate to analyze the influence of these variables on theudextraction kinetics and the oil quality obtained. Extraction curves are initially linear with a slope close toudthe oil solubility value in supercritical CO2. Based on these results a mathematical model was successfullyudapplied to describe the extraction curves. Characterization of supercritical crude corn oil was performedudby determining some physical parameters such as refraction index, density and color. Additionally, theudfatty acid composition, neutral lipids, the content of tocopherols, acid index, peroxide value, antioxidantudcapacity and the oxidative stability were determined in the corn oil extracted. Fatty acid composition wasudcompared with that for crude germ oil and no significant differences between the oils extracted by bothudmethods were found. Oxidative stability test using the Rancimat showed that supercritical CO2 extractedudcorn oil is less protected against oxidation than n-hexane extracted oils.
机译:这项工作已经研究了玉米胚芽油的超临界流体萃取。在不同的压力,温度和流速下进行萃取,以分析这些变量对萃取动力学和获得的油质的影响。提取曲线最初是线性的,其斜率接近/在超临界CO2中的油溶度值。基于这些结果,成功 udapply数学模型来描述提取曲线。通过确定一些物理参数(例如折射率,密度和颜色)来进行超临界玉米玉米油的表征。另外,测定了提取的玉米油中的脂肪酸组成,中性脂质,生育酚的含量,酸指数,过氧化物值,抗氧化剂能力和氧化稳定性。脂肪酸组成与粗制胚芽油的脂肪酸组成相比,两种方法提取的油之间没有显着差异。使用Rancimat进行的氧化稳定性测试表明,与正己烷萃取的油相比,超临界CO2萃取的 udcorn油对氧化的保护作用较小。

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