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Effect of incremental equal channel angular pressing (I-ECAP) on the microstructural characteristics and mechanical behaviour of commercially pure titanium

机译:等通道渐进角压制(I-ECAP)对商业纯钛微结构特征和力学行为的影响

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摘要

Incremental equal channel angular pressing (I-ECAP) is one of the continuous severe plastic deformation (SPD) processes. This paper presents the processing of commercial purity titanium (CP-Ti) using a double billet variant of I-ECAP process. Ultrafine-grain (UFG) structure was successfully achieved after six passes of I-ECAP at 300 °C. Microstructural evolution and texture development were tracked using EBSD. Analysis revealed continuous dynamic recrystallization (CDRX) as one of the grain refinement mechanism during processing. Room temperature tensile tests carried out before and after six passes, shows significant increase in strength with acceptable levels of ductility. The yield strength was increased from 308 to 558 MPa and ultimate tensile strength from 549 to 685 MPa. Compression tests conducted at different strain rates shows considerable increase in strength and enhanced strain rate sensitivity after processing. A distinct three-stage strain hardening was observed during compression. However the processed material displayed a loss in strain hardening ability during tensile as well as in compression tests. Detailed microhardness measurements show the evolution of hardness after subsequent passes with a reasonable level of homogeneity after the sixth pass. It is demonstrated that I-ECAP is an effective method for grain refinement in CP-Ti and subsequently improving its mechanical properties.
机译:等通道增量角压(I-ECAP)是连续严重塑性变形(SPD)过程之一。本文介绍了使用I-ECAP工艺的双方坯工艺加工商业纯度钛(CP-Ti)。 I-ECAP在300°C下经过6次通过后,成功实现了超细颗粒(UFG)结构。使用EBSD跟踪微观结构的演变和纹理的发展。分析显示,连续动态重结晶(CDRX)是加工过程中晶粒细化的机制之一。在六次通过之前和之后进行的室温拉伸试验显示出强度的显着提高以及可接受的延展性。屈服强度从308 MPa增加到558 MPa,极限抗拉强度从549 MPa增加到685 MPa。在不同的应变率下进行的压缩测试显示,加工后强度显着提高,应变率敏感性增强。在压缩过程中观察到明显的三阶段应变硬化。然而,加工过的材料在拉伸以及压缩测试中显示出应变硬化能力的损失。详细的显微硬度测量结果显示,随后的焊道经过第六次焊道后具有合理的均匀度,从而使硬度得以提高。事实证明,I-ECAP是在CP-Ti中细化晶粒并随后改善其机械性能的有效方法。

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