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[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate

机译：[（吡咯烷-1-基）碳硫基硫烷基]甲基吡咯烷-1-碳二硫酸酯

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摘要

The title compound, C11H18N2S4, was unexpectedly obtained during studies on the reactivity of the complex tris(acac-κ2 O,O′)gallium(III) (acac is acetylacetonate) with C4H8NCS2H in dichloromethane. The title compound shows disordered two pyrrolidine rings with major and minor occupancies of 0.546 (4) and 0.454 (4). Two (pyrrolidin-1-yl)carbothioylsulfanyl units are linked together through a methylene C atom and weak C—H⋯S interactions are found.

机译：在研究复杂的三（acac-κ2O，O'）镓（III）（acac是乙酰丙酮酸酯）与C4H8NCS2H在二氯甲烷中的反应性时，出乎意料地获得了标题化合物C11H18N2S4。标题化合物显示无序的两个吡咯烷环，主要和次要占据度分别为0.546（4）和0.454（4）。两个（吡咯烷基-1-基）碳硫基基硫烷基单元通过甲基碳原子连接在一起，并且发现弱的CHS相互作用。

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Chou, Wei-Lung; Yih, Kuang-Hway; Lee, Gene-Hsiang; Huang, Yen-Hsiang; Wang, Hsiao-Fen;
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年度 2010
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正文语种 {"code":"en","name":"English","id":9}
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专利

1. catena-Poly[[tris(4-fluorobenzyl)tin(IV)]-μ-2-[(piperidin-1-yl)carbothioylsulfanyl]acetato-κ2O:O′] [J] . Keng C.T., Lo K.M., Ng S.W. Acta Crystallographica Section E: Crystallographic Communications . 2010,第8期

机译：阳离子-聚[[三（4-氟苄基）锡（IV）]-μ-2-[（哌啶-1-基）碳硫基硫烷基]乙酰基-κ2O：O']
2. Comparison crystal structure conformations of two structurally related biphenyl analogues: 4,4′-bis[3-(pyrrolidin-1-yl)prop-1-yn-1-yl]-1,1′-biphenyl and 4,4′-bis{3-[(S)-2-methylpyrrolidin-1-yl]prop-1-yn-1-yl}-1,1′-biphenyl [J] . Wan A., Penthala N.R., Fifer E.K., Acta Crystallographica Section E: Crystallographic Communications . 2015,第10期

机译：两个结构相关联苯类似物的比较晶体结构构象：4,4'-双[3-（吡咯烷-1-基）丙-1-基-1-基] -1,1'-联苯和4,4'-双{3-[（（S）-2-甲基吡咯烷-1-基] prop-1-yn-1-yl} -1,1'-联苯
3. Comparison crystal structure conformations of two structurally related biphenyl analogues: 4,4′-bis[3-(pyrrolidin-1-yl)prop-1-yn-1-yl]-1,1′-biphenyl and 4,4′-bis{3-[(S)-2-methylpyrrolidin-1-yl]prop-1-yn-1-yl}-1,1′-biphenyl [J] . Wan A., Penthala N.R., Fifer E.K., Acta Crystallographica Section E: Crystallographic Communications . 2015,第10期

机译：两个结构相关联苯类似物的比较晶体结构构象：4,4'-双[3-（吡咯烷-1-基）丙-1-基-1-基] -1,1'-联苯和4,4'-双{3-[（（S）-2-甲基吡咯烷-1-基] prop-1-yn-1-yl} -1,1'-联苯
4. Study of the thermal, dielectric and mechanical properties of poly(methyl methacrylate-co-(1,4,7,10-tetraoxacyclododecan-2-yl)methyl methacrylate) membranes [C] . B. Redondo-Foj, P. Ortiz-Serna, M. Carsi Euromembrane Conference . 2013

机译：聚（甲基丙烯酸甲酯 - （1,4,7,7,10-四氧胞）甲基甲基丙烯酸甲酯甲基丙烯酸甲酯）膜的热，介电和力学性能研究
5. I:- Design, synthesis and study of nucleotide prodrugs. II:- Synthesis of 5-fluoro-6-[(2-aminoimidazol-1-yl)methyl]uracil (AIFU) and study of its mechanism of action as a thymidine phosphorylase inhibitor. III:- Design and synthesis of novel nucleotide analogs as alternative substrates for studying the mechanism of the thymidylate synthase-catalyzed reaction. [D] . Jain, Harsh Vardhan. 2010

机译：I：-核苷酸前药的设计，合成和研究。 II：5-氟-6-[（（2-氨基咪唑-1-基）甲基]尿嘧啶（AIFU）的合成及其作为胸苷磷酸化酶抑制剂的作用机理的研究。 III：-设计和合成新型核苷酸类似物作为研究底物胸苷酸合酶催化反应机理的替代底物。
6. (Pyrrolidin-1-yl)carbothioylsulfanylmethyl pyrrolidine-1-carbodithioate [O] . Wei-Lung Chou, Kuang-Hway Yih, Gene-Hsiang Lee, 2010

机译：（吡咯烷-1-基）碳硫基硫烷基甲基吡咯烷-1-碳二硫酸酯
7. catena-Poly[[tris(4-fluorobenzyl)tin(IV)]-μ-2-[(piperidin-1-yl)carbothioylsulfanyl]acetato-κ2 O:O′] [O] . Keng, Chun Thy, Lo, Kong Mun, Ng, Seik Weng 2010

机译：阳离子-聚[[三（4-氟苄基）锡（IV）]-μ-2-[（哌啶-1-基）碳硫基磺酰硫基]乙酰基-κ2 O：O′]

[(Pyrrolidin-1-yl)carbothio­ylsulfan­yl]methyl pyrrolidine-1-carbodithio­ate

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[(Pyrrolidin-1-yl)carbothioylsulfanyl]methyl pyrrolidine-1-carbodithioate