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Toward more realistic viscosity measurements of tyre rubber–bitumen blends

机译:为了更实际地测量轮胎橡胶-沥青混合物的粘度

摘要

The measurement of rheological properties of the tyre rubber bitumen blends is often challenging due to presence of suspended tyre rubber’s crumbs. Furthermore, the phase separation during the course of measurements makes the viscosity of these non-homogeneous blends difficult to ascertain. In this study, a new dual helical impeller was designed and manufactured to be used with a rotational viscometer in order to have a real-time control of the viscosity while performing a laboratory mixing of the blends. Layer based manufacturing techniques showed to be a convenient method to produce complex shaped impeller prototypes before manufacturing the more expensive stainless steel assembly. Impeller geometry was optimised to create a convective like flow within the sample and so minimise phase separation. Shear rate constant is geometry dependent and a calibration exercise was carried out to ascertain this. Results of both calibration and validation phases showed that the new impeller provides reliable viscosity measurements of homogenous fluids such as neat bitumen. With regards to complex fluids the new impeller showed a more stable and realistic trend than that obtained by using a standard spindle. In fact, it was demonstrated that the new impeller significantly decreases phase separation within the blend and in turns provides a more realistic measurement of the viscosity. This system represents a feasible and improved solution for optimising the laboratory modification process of tyre rubber bitumen blends by adapting the rotational viscometer as a low-shear mixer.
机译:由于存在悬浮的轮胎橡胶碎屑,因此轮胎橡胶沥青混合物的流变性能的测量通常具有挑战性。此外,在测量过程中的相分离使得难以确定这些非均匀共混物的粘度。在这项研究中,设计并制造了一种新的双螺旋叶轮,与旋转粘度计一起使用,以便在进行混合物的实验室混合时实时控制粘度。基于层的制造技术被证明是在制造更昂贵的不锈钢组件之前生产复杂形状的叶轮原型的便捷方法。叶轮的几何形状经过优化,可在样品内产生类似对流的流动,从而最大程度地减少相分离。剪切速率常数取决于几何形状,并进行了校准练习来确定这一点。校准和验证阶段的结果均表明,新型叶轮可对均质流体(如纯沥青)进行可靠的粘度测量。关于复杂流体,新叶轮比使用标准主轴显示出更加稳定和现实的趋势。实际上,事实证明,新的叶轮可显着降低共混物中的相分离,进而可提供更实际的粘度测量结果。该系统代表了一种可行且改进的解决方案,通过将旋转粘度计用作低剪切混合器来优化轮胎橡胶沥青混合料的实验室改性工艺。

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