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Rod-in-tube nanostructure of MgFe2O4: electrospinning synthesis and photocatalytic activities of tetracycline

机译:MgFe2O4的管中杆纳米结构:四环素的电纺合成及光催化活性

摘要

Magnesium ferrite (MgFe2O4) nanofibers were synthesized by direct annealing of electrospun precursor fibers using an appropriate heat treatment process. The crystal structure, morphology and surface area of the as-synthesized MgFe2O4 nanofibers were investigated by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy, respectively. The optical properties of the as-synthesized products were studied through ultraviolet-visible and photoluminescence spectroscopy. Due to its potential application in photocatalysis, the photocatalytic degradation of tetracycline (TC) was conducted, and the result indicated that MgFe2O4 showed a better photocatalytic degradation ratio (1.5 times and 2 times) of TC than the others under visible-light irradiation, which may be due to the unique rod-in-tube structure, and Larger specific area and the Larger specific surface area could absorb more catalyst and provide more active sites.
机译:通过使用适当的热处理工艺对电纺前驱体纤维进行直接退火,合成了铁氧体镁(MgFe2O4)纳米纤维。分别通过X射线衍射,扫描电子显微镜和透射电子显微镜研究了合成后的MgFe2O4纳米纤维的晶体结构,形态和表面积。通过紫外-可见光谱和光致发光光谱研究了合成产物的光学性质。由于其在光催化中的潜在应用,进行了四环素(TC)的光催化降解,结果表明,MgFe2O4在可见光照射下显示出比其他TC更好的TC的光催化降解率(分别为1.5倍和2倍)。可能是由于独特的管中杆结构,更大的比表面积和更大的比表面积可以吸收更多的催化剂并提供更多的活性部位。

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