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Preparation and Characterization of Alumina -Strontium Aluminate Based Composite

机译:氧化铝-铝酸锶基复合材料的制备与表征

摘要

Alumina-Strontium aluminate composites were prepared by mixing of Al2O3 and Sr(NO3)2 and calcination of powder at 1100oC. The calcined powder was compacted and sintered at 1600oC . The calcined powder XRD reveal that about 7% SrO. Al2O3 has formed in-situ in Al2O3. The sintered sample had poor relative density (75% of theoretical). The sintered samples were characterised for apparent porosity, bulk density, hardness, strength and toughness. The hardness of sintered sample was 2.49 GPa, bi-axial flexural strength was 37.3 MPa and Indentation Strength on Bending(ISB) fracture toughness of 1.7 MPam1/2. SEM microstructure of the sintered samples exhibit a porous microstructure. The strontium aluminate particles were seen as bright particles in phase contrast mode. The crack path was also viewed in SEM. It was noted that the cracks either were branched on interacting with strontium aluminate or stopped. This feature indicates the possibility of producing a tough sample if proper density and homogeneous distribution of Strontium aluminate could be achieved.
机译:氧化铝-铝酸锶复合材料是通过将Al2O3和Sr(NO3)2混合并在1100oC下煅烧粉末而制备的。将煅烧的粉末压实并在1600℃下烧结。煅烧粉末XRD显示出约7%的SrO。 Al2O3在Al2O3中原位形成。烧结样品的相对密度较差(理论值的75%)。烧结样品的特征在于表观孔隙率,堆积密度,硬度,强度和韧性。烧结样品的硬度为2.49 GPa,双轴弯曲强度为37.3 MPa,弯曲压痕强度(ISB)断裂韧性为1.7 MPam1 / 2。烧结样品的SEM显微组织显示出多孔的显微组织。在相衬模式下,铝酸锶颗粒被视为亮颗粒。在SEM中也观察到了裂纹路径。注意到,裂纹或者在与铝酸锶相互作用时分支或者停止。如果可以实现适当的密度和铝酸锶的均匀分布,则此特征表明可能会产生坚硬的样品。

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    Madhuchhanda Manali;

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  • 年度 2015
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