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Microstructure, magnetic and mechanical properties of Ni-Zn ferrites prepared by Powder Injection Moulding

机译:粉末注射成型法制备Ni-Zn铁氧体的组织,磁性和力学性能

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摘要

Nowadays, the electronic industry demands small and complex parts as a consequence of the miniaturization of electronic devices. Powder injection moulding (PIM) is an emerging technique for the manufacturing of magnetic ceramics. In this paper, we analyze the sintering process, between 900 °C and 1300 °C, of Ni–Zn ferrites prepared by PIM. In particular, the densification behaviour, microstructure and mechanical properties of samples with toroidal and bar geometry were analyzed at different temperatures. Additionally, the magnetic behaviour (complex permeability and magnetic losses factor) of these compacts was compared with that of samples prepared by conventional powder compaction. Finally, the mechanical behaviour (elastic modulus, flexure strength and fracture toughness) was analyzed as a function of the powder loading of feedstock. The final microstructure of prepared samples was correlated with the macroscopic behaviour. A good agreement was established between the densities and population of defects found in the materials depending on the sintering conditions. In general, the final mechanical and magnetic properties of PIM samples were enhanced relative those obtained by uniaxial compaction.
机译:如今,由于电子设备的小型化,电子工业需要小型且复杂的零件。粉末注射成型(PIM)是制造磁性陶瓷的新兴技术。在本文中,我们分析了PIM制备的Ni-Zn铁氧体在900°C至1300°C之间的烧结过程。特别是,在不同温度下分析了具有环形和棒形几何形状的样品的致密性,微观结构和力学性能。另外,将这些压块的磁性能(复磁导率和磁损耗因子)与通过常规粉末压制制备的样品的磁性能进行了比较。最后,分析了机械性能(弹性模量,弯曲强度和断裂韧性)与原料粉末装载量的关系。制备样品的最终微观结构与宏观行为相关。在材料的密度和缺陷总数之间建立了良好的协议,这取决于烧结条件。通常,PIM样品的最终机械和磁性能相对于通过单轴压实获得的机械和磁性能有所提高。

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