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Influence of Deposition Parameters and Thermal Annealing on the Structure and Properties of Nitride Coatings (TiHfZrVNb)N

机译:沉积参数和热退火对氮化涂层(TiHfZrVNb)N的结构和性能的影响

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摘要

Results of structure, phase composition, physical and mechanical properties and tribological properties investigations of nitride high-entropy coatings (TiZrHfVNb)N are presented in the paper. Proton microbeam (m-PIXE), X-ray diffraction method, including method of X-ray strains measurements, energy dispersive X-ray spectroscopy and scanning electron microscopy analysis, microhardness testing and nanoindentation were used. Thermal annealing (t = 600 C) influence on defect profiles, structure and element distribution in the coatings was investigated. It was found that thermal treatment of coatings leads to changing of defect profiles and to element redistribution.Also we can say that it influences less on grain size changing. Investigated (TiZrHfVNb)N coatings demonstrate high values of hardness and excellent wear resistance.
机译:本文介绍了氮化物高熵涂层(TiZrHfVNb)N的结构,相组成,物理力学性能和摩擦学性能的研究结果。使用了质子微束(m-PIXE),X射线衍射法,包括X射线应变测量方法,能量色散X射线光谱法和扫描电子显微镜分析,显微硬度测试和纳米压痕。研究了热退火(t = 600 C)对涂层中缺陷轮廓,结构和元素分布的影响。发现涂层的热处理会导致缺陷轮廓的改变和元素的重新分布,也可以说它对晶粒尺寸变化的影响较小。研究的(TiZrHfVNb)N涂层显示出较高的硬度值和出色的耐磨性。

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