Trace levels of cyanide were found in the effluent wastewater resulting from the production of dinitrotoluene. To determine the source of cyanide, a survey of the system was conducted. The wastewater treatment plant was also surveyed before and during dinitrotoluene production.Iso-octane extraction, exposure to ultraviolet light, and metal sequestering agents were used in attempts to perform these analyses. These methods did not give consistent results; therefore, the conventional distillation method followed by colorimetric or selective ion electrode determination was used.
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