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SINTESIS DAN KARAKTERISASI NANOPARTIKEL PERAK DENGAN METODE PULSED LASER ABLATION IN LIQUID (PLAL)

机译:脉冲激光烧蚀液相法制备银纳米粒子及其表征

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摘要

Synthesis of Silver Nanoparticles by Pulsed Laser Ablation in Liquid (PLAL) with variation of time, laser wavelengths, energy, concentration, and variation of dispersants has been investigated. Colloidal nanoparticles with optimum absorbance were obtained by pulsed laser Nd: YAG with 532 nm wavelength, the laser pulse energy of 30 mJ, at a repetition rate 10 Hz, 0.01 wt% PVP as 10 mL with irradiation for 40 min respectively. UV???visible absorption, Particle Size Analyzer and Transmission Electron Microscope were justed for the characterization of Silver Nanopartical (NPs). The absorption spectra of the colloids showed that a plasmon absorption peak was around 400 nm. Transmission Electron Microscopy demonstrated that the obtained nanoparticles were spherical with average size varying from 6.4 nm to 19.2 nm. The average of diameter and distribution of Ag-NPs particles significantly depends on parameters.
机译:已经研究了在时间,激光波长,能量,浓度和分散剂的变化下,通过脉冲激光烧蚀液体(PLAL)合成银纳米粒子的方法。通过以532 nm波长的脉冲Nd:YAG脉冲激光,30 mJ的激光脉冲能量,10 Hz的重复频率,10 wt的0.01 wt%PVP照射40分钟,获得具有最佳吸收率的胶体纳米颗粒。用紫外可见吸收,粒度分析仪和透射电子显微镜表征银纳米颗粒(NPs)。胶体的吸收光谱表明,等离激元吸收峰在400nm左右。透射电子显微镜证实,所获得的纳米颗粒是球形的,平均尺寸在6.4nm至19.2nm之间变化。 Ag-NPs颗粒的直径和分布的平均值明显取决于参数。

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    Mujtahid Fitriah;

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  • 年度 2017
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