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Effect of new sealing treatments on corrosion fatigue lifetime of anodized 2024 aluminium alloy

机译:新型密封处理对阳极氧化2024铝合金腐蚀疲劳寿命的影响

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摘要

The effect of two sealing processes, i.e. an usual hydrothermal sealing and an innovating sealing process called (B1 + B2), on fatigue behavior of anodized AA2024 was studied in air for as prepared and pre-corroded samples. Pre-corrosion exposure corresponded to salt-spray tests or continuous immersions. For salt-spray tests, the best corrosion resistance was related to the (B1+B2) sealing and, for continuous immersions, to the hydrothermal sealing. Fatigue life tests in air on pre-corroded samples revealed that anodized samples presented a decrease in fatigue life more pronounced than anodized and sealed samples in relation with a lower corrosion resistance; fatigue crack initiation was localized on pits issued from the degreasing and pickling steps. Independent of the sealing process, the fatigue behavior of the anodized and sealed samples depended on the pre-corrosion exposure. Corrosion fatigue tests induced an additional decrease in fatigue life for both sealing treatments. Crack initiation occurred preferentially on pits issued from degreasing and pickling but also on pits issued from interaction between cyclic loading and corrosive media, in relation with amechanical damage of the sealed anodic film. The differences in sealed layer morphology could explain the difference in fatigue resistance between the sealed anodic films.
机译:对于准备和预腐蚀的样品,研究了两种密封工艺,即通常的水热密封和称为(B1 + B2)的创新密封工艺对阳极氧化AA2024疲劳行为的影响。腐蚀前暴露对应于盐雾测试或连续浸没。对于盐雾测试,最佳的耐腐蚀性与(B1 + B2)密封有关,对于连续浸没,与水热密封有关。在空气中对预腐蚀样品的疲劳寿命测试表明,与较低的耐蚀性相比,阳极氧化的样品与阳极氧化和密封的样品相比,疲劳寿命的降低更为明显。疲劳裂纹的产生局限于脱脂和酸洗步骤中产生的凹坑。与密封过程无关,阳极氧化和密封样品的疲劳行为取决于预腐蚀暴露。两种密封处理的腐蚀疲劳试验均导致疲劳寿命进一步降低。与密封阳极膜的机械损伤有关,裂纹萌生优先发生在除油和酸洗所产生的凹坑上,但也发生在周期性载荷与腐蚀性介质之间的相互作用所产生的凹坑上。密封层形态的差异可以解释密封阳极膜之间的抗疲劳性差异。

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