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Project of method developing of quality control of spruce essential oil by gas-liquid chromatography

机译:气液色谱法云杉精油质量控制方法开发项目

摘要

Conditions of the chromatography analyses of essential oils providing the yield of all components with the contents over 0.01% were selected. Essential oils of 10 samples of Norway spruce growing inthe same edaphic-climatic conditions of the park UE “Brovki” were obtained by hydrodistillation. Qualitative and quantitative analyses of the received essential oils were performed. More than 50 components composing the essential oil were identified. The obtained statistic data allowed to calculatestandard deviation of repeatability, standard deviation of intermediate precision with a variable factor “time + operator”, expanded uncertainty of measurement results for the confidence level P = 0,95.
机译:选择精油色谱分析的条件,以提供含量超过0.01%的所有组分的收率。通过加氢蒸馏获得了在UE“ Brovki”公园相同的气候条件下生长的挪威云杉的10个样品的精油。对收到的精油进行定性和定量分析。鉴定出超过50种组成精油的成分。获得的统计数据可用于计算重复性的标准偏差,具有可变因子“时间+算子”的中间精度的标准偏差,置信度P = 0.95时测量结果的不确定性。

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